Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A

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Some specific hazards statements are given in Work Item s – proposed revisions of this standard. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. The bent samples are examined at low magnification, where the a622 of cracks or fissures indicate intergranular attack.

ASTM does not give any warranty express or implied or make any representation that the contents of this abstract are accurate, complete or up to date.

In everyday applications, corrosion varies by materials and solutions. This method is a hour boiling test for “as received” specimens of stainless steel. The Copper Sulfate Test is especially effective for determining susceptibility to intergranular attack practie low carbon steels. The test is generally performed for acceptance of materials, but not sufficient for rejection of materials.

In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away. The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly oxidizing environments such as nitric acid. It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with practive precipitation of chromium carbides at grain boundaries.


Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals. The oxalic acid test is commonly used before the Strauss test to determine if a sample is susceptible; samples that pass method A will generally show low corrosion rates in the Strauss test.

It depends on which Practice is selected, but typically ranges from to days for different pracrice. Methods for preparing the test specimens, rapid screening tests, apparatus setup and testing procedures, and calculations and report contents are described for each testing practice.

Historical Version s – view previous versions of standard.

Please refer to the specification for more details. We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments.

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This simple etching technique is used as a quick screening method to ensure aastm a material is free of intergranular corrosion susceptibility. The samples are weighed at each interval to determine mass loss and degree of susceptibility prractice intergranular attack.

It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior.

ASTM A testing is a popular method of choice due to the variety of practices available and the relatively short turnaround for results.

Corrosion Testing

Please specify the maximum allowable corrosion prractice and any available data on the sensitizing heat treatment performed. The etch structure types used to classify the specimens are: Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion practide testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.


This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively. However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur. Share on Tumblr Print. Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels.

See Appendix X1 for information regarding test selection. Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries.

For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions. A bend test followed by a visual or micro-examination are used to pactice “Pass” or “Fail” of test specimens. It is informational only and not an official part of the standard; the full text of the standard itself must be referred to for its use and application. For example, many low-carbon and stabilized stainless steels e.

Intergranular Corrosion Testing: An Overview of ASTM A262

The inch-pound equivalents are in parentheses and may be approximate. Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on.

Strauss test specimens are practce in a Copper Sulfate – Sulfuric Acid mixture for 15 hours. Sensitization causes the grain boundaries of a material to precipitate, creating carbide deposits and causing the material to be susceptible to intergranular attack.